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The drives are only accessible through the Caltech on campus network or VPN.
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Many users get their data from a global shared drive, although if you prefer, you can choose to exclude your data from this drive and have an individual password protected drive containing just your data.
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The principal way you can retrieve your data to process it or back it up on your own computer is through Windows read-only network drives, which also work with Apple software.
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We have a site license for the MestReNova NMR software, and encourage all lab users to install it on their own computers and become familiar with it. if you will be attempting an experiment you have little familiarity with, don't do it in the middle of the night when it is very unlikely you can get any help. Exercise some judgment when you plan your experiments-e.g. If the problem means that the instrument is not usable, leave a note on the workstation saying the instrument is down. After hours, you may call or look for the instrument GLA in their lab, but if you cannot reach them, send an email or text to them (also copy Dave on the email). If you have a problem with an instrument, and it is during business hours, attempt to contact Dave first and then the instrument GLA. Knowing and adhering to the signup rules is the responsibility of the user.Įach instrument has a written log book, where you should enter your initials and your advisor's initials, lab phone extension, starting and ending time, nuclei and solvent, and any problems you encountered.
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The instrument automation software will enforce some, but not all, of the signup rules. Webcal does not enforce any scheduling rules when reservations are made. During the day, do not sign up on webcal for those instruments. We only use the webcal schedules on those three instruments during the night queue, in order to make sure that the night queues do not get overbooked. The automated instruments hg3, indy, florence, and verona on automation days are run under automation software and maintain their own first come, first served schedules.
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Verona should be scheduled on webcal on the days when it is in manual mode, or for the night queue. The instruments which should be scheduled on webcal at all times are fid, siena, and hg2. Instrument scheduling is done as needed on a Webcal schedule, for instance this one for siena (the others are analogous): Those are summarized on the Instruments page, and the GLA will cover them during your training session. You can subscribe here: Įach instrument has a specific signup/reservation/acceptable use policy. This mailing list is how we inform users about instruments that are down, when they come back up, new software, lab policy changes, etc. There is one training for the automated instruments indy and fid-at the conclusion, you will get user accounts on both instruments.Īt the time you sign up for your first training session, subscribe to the NMR users mailing list. Also, we have found that new users progress faster if they get trained on one instrument, then practice until they gain competence before moving on to another instrument. We ask that users sign up for training on only one instrument at a time otherwise, it can become very unclear what the sequence of training sessions is going to be. If there isn't a training session already scheduled for the instrument you are interested in, the GLA should contact you to schedule one. You will also find a list of any currently scheduled training sessions there, and GLA contact information. To request new user training, sign up on the white board just inside the NMR lab main door. If your PTA number changes, inform Dave what the new number is. Return this completed form to the GLA or to Dave before using the instrument for the first time. The "PTA alias" which is a letter P followed by a 5-6 numbers is not valid. The PTA will normally begin with your advisor's initials. As part of the training, you will receive and complete a form acknowledging your understanding of the lab safety rules, and entering the PTA (Caltech internal accounting number) to which your NMR bills will be charged. Instrument users should receive training from a GLA before running any of the instruments. Authorized users should not bring visitors with them inside any marked 5 gauss line. The high magnetic field areas should only be entered by authorized instrument users who have completed new user safety training (see below), and do not have cardiac pacemakers or other risk factors. These areas are marked on the floor with red and white striped tape.
Past that line, there are areas around each NMR magnet where the stray magnetic field exceeds 5 gauss. The lab is open for visits or tours from the main door up to the yellow line in the floor tile.
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